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Monday, December 29, 2014

#201 - Top 10 Nova Blog Posts from 2014

Probably everyone does a year-end post about what content was most popular on their blog. The areas of interest sometimes indicate an explainable trend, and sometimes they don’t. Nova is a technical company that manufactures analytical instruments. So our audience tends to be of the engineering and analytical types.

Our top 10 posts from 2014 are the following:

1. Post #167 - Using the Energiron Process with SynGas for DRI Production
2. Post #169 - Most Common Connections to Nova Analyzers (electrical & tubing)
3. Post #175 - Tenova Factories
4. Post #171 - New TGI White paper - Real-Time Water Detection in EAF Steelmaking
5. Post #173 - Nova tech climbs Mount Kilimanjaro
6. Post #168 - Nova Analyzers from the Field – Episode 4
7. Post #172 - Ash Classification Technology for Coal-fired Power Plants
8. Post #174 - Nova Analyzers from the Field – Episode 5
9. Post #178 - Nova Analyzers from the Field – Episode 6
10. Post #182 - Oil & Gas Spills Increase in 2013

For the most part, these posts from 2014 have simply accumulated higher popularity because they are from the first half of the year and are obviously older than any recent posts.

In terms of persistent interest, our ‘Analyzers from the Field’ posts seem to do well. People are always interested in reading about something ‘real world’. Frequently, these instruments have been in service for a number of years and have some kind of back-story that may be instructive.

Regarding Post #173 mentioned above, in May of 2014, one of our tech staff ventured to Africa to climb Mount Kilimanjaro. Lots of readers from inside and outside the Tenova Group were interested to hear the story and see the pictures. We still have tons of pics besides what we posted. We'll share a few more soon. 

Our all-time #1 post continues to be Post #70 - "Post #5 is our most popular blog post (Syngas and Gasification)". This one started out as a commentary on another popular post and then itself became most widely read. It indicates the continued interest in measuring the gas compositions produced by gasifiers.

Looking forward to 2015!

For information on these and other gas analyzer systems, give Mike or Dave at Nova a call, or send us an e-mail.

If you have any Nova instruments at your plant or lab and want to share a couple of photos, feel free to send them to us along with a brief explanation of your application.

1-800-295-3771
sales at nova-gas dot com
websales at nova-gas dot com
http://www.nova-gas.com/

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Thursday, December 18, 2014

#200 - Nova Analyzers from the Field - Episode 9 (Studies of CO2 Absorption / Desorption by Amine Solutions)

We were recently sent a published paper containing a brief mention of a Nova analyzer. The paper itself is about the kinetics of CO2 absorption in various aqueous amine solutions. We have periodically addressed this type of application over the years. As carbon dioxide (CO2) becomes more prominently connected with concerns about greenhouse gases, we expect to see more of it in the future also.

From the Introduction of the paper: 
“The separation of acid gas impurities such as carbon dioxide (CO2) and hydrogen sulfide (H2S) from gas mixtures is an important operation in natural gas processing, petroleum refining, coal gasification and ammonia manufacturing industries. Since CO2 is widely regarded as a major greenhouse gas, potentially contributing to global warming, recently, there has also been considerable interest in developing technologies for capturing and sequestering large quantities of CO2 produced from industrial sources such as fossil-fuel electric power generation facilities. Various technologies have been developed for CO2 and H2S removal from gas streams. These include absorption by chemical and physical solvents, cryogenic separation and membrane separation. Among these methods, gas absorption by chemical solvents such as aqueous solutions of alkanolamines is one of the most popular and effective methods.”

Even though this area of study has been active and applied in industry for over 50years, the authors note that complete investigations with mathematical models for absorption and desorption have been lacking. The authors then present a more unified approach in an effort to allow more standardized evaluations of this application across different reactions.

In this study, a novel design of laboratory contactor apparatus was used for interfacial contact between the amine and CO2. This apparatus allows for accurate and easier evaluation of physical mass transfer between the reactants. A diagram of the apparatus as presented in the paper is shown below.



The complete experimental setup from the paper is shown below:



After the dryer and just prior to the fume hood, the CO2 analyzer is shown in the above setup diagram. In this particular study the authors cite the Nova Model 300 infrared analyzer. In our experience, we have supplied a couple of different instruments for this type of application.
-          Model 302A – CO2 analysis by infrared detector
-          Model 336BT – CO2 analysis by thermal-conductivity (not shown in on-line catalog)

In one application in 2013, we supplied multiple units of Model 336BT in two ranges:
-          0-25.0 % CO2 in Air
-          0-100.0 % CO2 in Air

This application was for a large educational training assembly that involved the same absorption reactions between amine & CO2 mentioned above. The different instrument ranges corresponded to different points in the process before & after CO2 absorption. Purchasing separate instruments allowed simultaneous measurement of each point over a specific period of time.

In most cases, these studies are performed using portable instruments that provide accurate analysis on a temporary / intermittent basis. A wall-mounted version of this instrumentation can also be produced. For study apparatuses that are large enough to be permanently installed, a wall-mount analyzer in its own steel cabinet may be desired.



The study mentioned above is actually described in a two part paper as follows:

Part 1
Kinetics of carbon dioxide absorption and desorption in aqueous
alkanolamine solutions using a novel hemispherical contactor—I:
Experimental apparatus and mathematical modeling.

Part 2
Kinetics of carbon dioxide absorption and desorption in aqueous alkanolamine solutions using a novel hemispherical contactor—II: Experimental results and parameter estimation

Authors:
Aqil Jamal
Axel Meisen
C. Jim Lim
Department of Chemical and Biological Engineering,
The University of British Columbia
Vancouver, BC Canada V6T 1Z3


For information on these and other gas analyzer systems, give Mike or Dave at Nova a call, or send us an e-mail.
1-800-295-3771
sales at nova-gas dot com
websales at nova-gas dot com

Hey, this is Post #200 in our blog. Still haven’t run out of things to say!


Author: Aqil Jamal, Axel Meisen and C. Jim Lim
Publication: Chemical Engineering Science
Publisher: Elsevier
Date: October 2006
Copyright © 2006 Elsevier Ltd.
All rights reserved.
* Experiment diagrams and information property of authors

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Friday, December 12, 2014

#199 - Why Buy 970?

The most popular post on this blog is #70, which is ironically entitled “Post #5 is Our Most Popular Blog Post”. Post #70 was intended to highlight the previous successful post #5 that discussed the growing interest in our 970 Series analyzers for syngas applications.

These posts are probably so popular because there is much world-wide interest in gasification as an energy source. These posts contain specific information and pictures about gas analyzers that can successfully measure O2 / CO / CO2 / CH4 / H2 in produced syngas.

We are often asked questions about the price and configuration of the 970 Series. We do have instruments in our product line that are much smaller and simpler (as pictured below). There are other analyzer manufacturers in the marketplace that also have multi-gas capability like Nova, but who are possibly lower-cost. For a gasification application, is it simply a matter of obtaining an analyzer that will measure the gases of interest?




Not always. Gas analysis is usually only the second half of the whole task. The first half involves extracting the sample, filtering it, and drying it. Doing this properly in a syngas application is important.

There is an old saying about comparing ‘apples to apples’. When we are asked to compare the 970 to another analyzer that resembles the picture above, the first thing that we notice is that all of the sample extraction and conditioning components are missing. Unless the end-user is absolutely confident that the produced gas is clean and dry, this style of instrument will not function properly for very long. Trust us - we have learned that lesson the hard way in the past.

The Nova 970 Series Syngas and Gasification Analyzers are analytical instruments that are industrially hardened but user-friendly.
  • High temp probe & heated filter at extraction point.
  • Choice of compression or thermoelectric style moisture removal.
  • Weather-proof cabinet with climate control.
  • Stainless steel tubing and industrial components.
  • Temperature-controlled detectors for O2 / CO / CO2 / CH4 / H2
  • Accurate H2 measurement in varying background gases.
  • High measurement ranges available; up to 100%.
  • Built-in ‘Smart Control’ analyzer functions




Here is some more information plus a link to the 970 section of the catalog. 

For information on these and other gas analyzer systems, give Mike or Dave at Nova a call, or send us an e-mail.
1-800-295-3771
sales at nova-gas dot com
websales at nova-gas dot com
http://www.nova-gas.com/